product name: fmoc-phe(4-cf3)-oh lot no.: gls170420-23725

cas no.: 247113-86-6 store at: cool dry place(<25oc)

molecular formula: c25h20f3no4 molecularweight: 455.43

manufacturing date: 2017-4-20 retest date: 2019-4-20

melting point: 134.4oc specific rotation[a]20

d: -37.7o(c=1 in dmf)

tests specifications results

appearance

purity(hplc)

clarity of solution

water content(k.f.)

loss on drying

ir spectrum

mass spectrum

nmr spectrum

white to off white powder

≥98%

0.3 gram in 2ml dmf clear solution

≤2.0%

≤2.0%(70oc,2h)

in accordance with the structure

in accordance with the structure

in accordance with the structure

complies

99.08%

complies

0.90%

0.44%

complies

complies

complies

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